Zita: | Ethyl 4-bromobutyrate |
Shoko rakafanana: | 4-Bromobutanoic acid, ethyl ester;BRCH2CH2CH2C(O)OC2H5; Butanoic asidhi, 4-bromo-, ethyl ester;Ethyl 4-bromobutanoate; Ethyl gamma-bromobutyrate;ETHYL 4-BROMO-N-BUTYRATE; ETHYL GAMMA-BROMO-N-BUTYRATE |
CAS: | 2969-81-5 |
Formula: | C6H11BrO2 |
Chitarisiko: | Mvura yero zvishoma |
EINECS: | 221-005-6 |
HS Kodhi: | 2915900090 |
Mubhodhoro rekuita rakashongedzerwa nestirrer, thermometer uye vent chubhu, 200 g (2.33 mol) ye γ -butyrolactone uye 375mL yeanhydrous ethanol yakawedzerwa, yakatonhodzwa kusvika 0 ℃ muchando chekugezesa munyu, uye yakaomeswa hydrogen bromide gasi yakaunzwa kusvika. mareactants akaramba asina kuchinjwa, izvo zvakatora maawa maviri.Isiye pa 0 ℃ kwe 24h.Dururira reactant mu 1L mvura inotonhora, simbisa zvizere, paradzanisa organic layer, uye bvisa iyo mvura layer ne bromoethane kaviri, 10mL nguva imwe neimwe.Kubatanidza organic layers, kugeza ethanol ne2% potassium hydroxide solution, dilute hydrochloric acid nemvura, kuomesa neanhydrous sodium sulfate, kupora solvent, vacuum fractionating, uye kuunganidza zvikamu pa97 ~ 99℃/3.3 kPa kuwana 350 ~ 380 g yeethyl γ-bromobutyrate (1) ine goho re77% ~ 84%.
Ethyl 4- bromobutyrate inotorwa necarboxylate, isina ruvara, inoonekera kune yero mvura.Inogona kushandiswa sepakati pemishonga yezvipembenene nemishonga, uye inogona kushandiswa mukutsvagisa marabhoritari nekusimudzira uye kugadzirwa kwemakemikari.
Kurongedza Giredhi: I;II
Chikamu cheNjodzi: 6.1
HS Kodhi: 2915900090
WGK_Germany (Kuronga Rondedzero yeZvinhu Zvinosvibisa Mvura muGermany): 3
Hazard Kirasi Code: R22;R36/37/38
Mirayiridzo Yekuchengetedza: S26-S36-S37/39
Chiratidzo chekuchengetedza: S26: Kana wasangana nemaziso, sukurudza nekukurumidza nemvura yakawanda uye utumire kuna chiremba.
S36: Pfeka zvipfeko zvinodzivirira zvakakodzera.
Hazard Signs: Xn: Inokuvadza